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Cost-effective and customizable 2',3',4'-TRIMETHOXYACETOPHENONE 13909-73-4 factory
- Molecular Formula: C11H14O4
- Molecular Weight: 210.23
- Appearance/Colour: clear yellow liquid
- Melting Point: 14-15 °C(lit.)
- Refractive Index: n20/D 1.5384(lit.)
- Boiling Point: 295.999 °C at 760 mmHg
- Flash Point: 133.739 °C
- PSA： 44.76000
- Density: 1.089 g/cm3
- LogP: 1.91500
13909-73-4 Relevant articles
An unusual anodic methoxylation: 3,4-dimethoxyacetophenone
Hawkes,Hawkes,Comninos,Pardini,Viertler
, p. 8133 - 8136 (1992)
The electrolysis of 3,4-dimethoxyacetoph...
Tropylium Ion Catalyzes Hydration Reactions of Alkynes
Oss, Giulia,Ho, Junming,Nguyen, Thanh Vinh
supporting information, p. 3974 - 3981 (2018/08/17)
The hydration of alkynes is one of the m...
Novel 2,4,5-trisubstituted oxazole derivatives: Synthesis and antiproliferative activity
Liu, Xin-Hua,Lv, Peng-Cheng,Xue, Jia-Yu,Song, Bao-An,Zhu, Hai-Liang
experimental part, p. 3930 - 3935 (2009/12/04)
Microwave irradiation promotes the rapid...
Miscrowave-assisted efficient synthesis of polymethoxyacetophenones and natural polymethoxyflavones, and thier inhibitory effects on melanogenesis
Tsukayama, Masao,Kusunoki, Eiji,Hossain, Mohammad M.,Kawamura, Yasuhiko,Hayashi, Shinji
, p. 1589 - 1600 (2008/09/17)
Microwave, assisted Friedel-Crafts acety...
FLAVONES
-
Page/Page column 18; 49, (2008/06/13)
The present invention relates to flavone...
13909-73-4 Process route
-
-
528-21-2
2',3',4'-trihydroxyacetophenone
-
-
77-78-1
dimethyl sulfate
-
-
13909-73-4
2',3',4'-trimethoxyacetophenone
| Conditions | Yield |
|---|---|
|
With
potassium carbonate;
In
acetone;
for 24h;
Heating;
|
90.5%
|
|
2',3',4'-trihydroxyacetophenone; dimethyl sulfate;
With
potassium carbonate;
In
acetone;
at 45 ℃;
for 17h;
With
water;
In
acetone;
|
85%
|
|
cetyltrimethylammonim bromide;
In
sodium hydroxide; chloroform;
Ambient temperature;
|
80%
|
|
With
aqueous alkali;
|
-
-
634-36-6
1,2,3-trimethoxybenzene
-
-
108-24-7
acetic anhydride
-
-
13909-73-4
2',3',4'-trimethoxyacetophenone
| Conditions | Yield |
|---|---|
|
With
PPA;
|
80%
|
|
With
In(OSO2CF3)3;
at 75 - 90 ℃;
for 0.116667h;
Irradiation;
Microwave;
|
73%
|
|
silver hexafluoroantimonate; bis(benzonitrile)dichloroplatinum(II);
In
dichloromethane;
Heating;
|
62%
|
|
With
perchloric acid; acetic acid;
|
|
|
With
PPA;
at 45 ℃;
|
13909-73-4 Upstream products
-
634-36-6
1,2,3-trimethoxybenzene
-
108-24-7
acetic anhydride
-
75-36-5
acetyl chloride
-
64-19-7
acetic acid
13909-73-4 Downstream products
-
859076-87-2
1-(2,3,4-trimethoxy-phenyl)-3-(3,4,5-trimethoxy-phenyl)-propane-1,3-dione
-
858834-56-7
1-(3,4-dimethoxy-phenyl)-3-(2,3,4-trimethoxy-phenyl)-propane-1,3-dione
-
5396-18-9
2'-hydroxy-3',4'-dimethoxyacetophenone
-
62615-26-3
1-(2,4-dihydroxy-3-methoxyphenyl)ethan-1-one
